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Silica-Supported ICI as a novel Hetergenous System for the Rapid Oxidation of Urazoles to Triazolinediones

ICl–SiO2 as a new reactive system was prepared by the treatment of iodine monochloride with an activated silica gel in chloroform. ICl–SiO2 in a heterogeneous system efficiently oxidized urazoles to the corresponding triazolinediones under mild conditions in high yields at room temperature.

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